Calcium leaching in the samples treated with N2 saturated brine was found to be a thermally dependent process; in fact the activation energy for Ca transport was found to be higher when increasing temperature from 60C to 120C. At temperatures higher than 60C full conversion of portlandite to other forms was justified on the grounds of activation energy and appeared to cause chemical instabilities within the grouts. Those instabilities where aggravated in the case of the carbonated brine.The examined carbonated samples showed two clearly defined areas (inner core and carbonated region) for any duration, that were separated by a clear demarcation line, namely the carbonation front.
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